Journal of Prosthetic Dentistry
Volume 88, Issue 4 , Pages 396-401, October 2002

Light-polymerized compomers: Coefficient of thermal expansion and microhardness☆☆★★

College of Dentistry, Kyungpook National University, Taegu, Korea; and University of Texas Health Science Center at San Antonio, San Antonio, Texas

Abstract 

Statement of Problem. The relationship between the filler content, coefficient of thermal expansion, and microhardness of commercial light-polymerized compomers has not been fully investigated. Purpose. This study evaluated the effect of filler content on the coefficient of thermal expansion and microhardness of 3 commercially available light-polymerized compomers. Material and Methods. Five specimens each from 3 commercially available compomers (Compoglass F, Elan and F2000) were evaluated. Linear thermal expansion (μm/°C) was measured with a thermomechanical analyzer in the temperature range 20° to 80°C with increments of 10°C. Standardized specimens were prepared in a metal die (1.5 × 2 × 12 mm) and polymerized for 40 seconds at 700 mW/cm2 light intensity. The microhardness of 5 specimens from each of 3 compomers were measured with a Vickers hardness tester under a 15-second dwell time and 200-g load conditions. The specimens were polymerized at 700 mW/cm2 intensity for 40 seconds after placing the compomers into a round aluminum mold. Differences in thermal expansion and microhardness among the compomers evaluated were statistically analyzed by use of one-way analysis of variance at P<.01 significance level, with differences assessed by use of Duncan's multiple range post hoc test. Results. The coefficients of thermal expansion of Compoglass F (54.17 ± 0.54 μm/°C), Elan (40.94 ± 0.78 μm/°C) and F2000 (24.43 ± 89 μm/°C) were almost linear in the temperature range 25° to 80°C for all 3 compomers (r >.99). Inverse correlations between the %wt of filler and the coefficient of thermal expansion (r = −0.98, P<.0001), as well as between the microhardness and the coefficient of thermal expansion (r = −0.98, P<.0001) were observed. On the other hand, a linear correlation between the %wt of filler and microhardness of compomers was exhibited (r = −0.96, P<.0001). The microhardness values for Compoglass F, Elan, and F2000 were 43.82 ± 1.62, 58.16 ± 1.90, and 72.94 ± 3.29, respectively. Conclusion. Within the limitations of this study, an inverse correlation between percent weight of filler and coefficient of thermal expansion, and a linear correlation between percent weight of filler and microhardness was observed for the evaluated compomers. (J Prosthet Dent 2002;88:396-401.)

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 Reprint requests to: Dr. Kyo-Han Kim, Kyungpook National University, College of Dentistry, Department of Biomaterials 700-422, Taegu KOREA, Fax: (82) 53-422-9631, E-mail: kyohan@knu.ac.kr

☆☆ aResearcher, Department of Dental Biomaterials and Institute for Biomaterials Research and Development, Kyungpook National University, College of Dentistry.

 bGraduate Student, Department of Dental Biomaterials, Kyungpook National University, College of Dentistry.

★★ cAssociate Professor, Department of Restorative Dentistry, Division of Biomaterials, University of Texas Health Science Center at San Antonio.

 dProfessor and Director, Department of Dental Biomaterials and Institute for Biomaterials Research and Development, Kyungpook National University, College of Dentistry; Visiting Professor, Department of Restorative Dentistry, Division of Biomaterials, University of Texas Health Science Center at San Antonio.

PII: S0022-3913(02)00231-7

doi:10.1067/mpr.2002.128121

Journal of Prosthetic Dentistry
Volume 88, Issue 4 , Pages 396-401, October 2002